Freitag, 26. Februar 2016

Repeated dose toxicity: dermal.001

Repeated dose toxicity: dermal.001


Administrative data

Study result type:
experimental result
Reliability:
4 (not assignable)
Rationale for reliability incl. deficiencies:
Alcide gel was used in this study (antimicrobial compound consisting of solutions of sodium chlorite and lactic acid that produce chlorine dioxide when mixed)

Data source

Reference
Reference Type:
publication
Title:
Pharmacodynamics of Alcide, a new antimicrobial compound, in rat and rabbit
Author:
Scatina JA, Abdel-Rahman MS, Gerges SE, Khan MY and Gona O
Year:
1984
Bibliographic source:
Fundamental and Applied Toxicology, 4: 479-484

Materials and methods

Test guideline
Qualifier:
no guideline followed
Principles of method if other than guideline:
The dermal toxicity of Alcide gel was assessed following application of the gel to the backs of rabbits 5 days/week for 3 months.
GLP compliance:
no data
Test type:
subchronic
Limit test:
no

Test materials

Identity of test material same as for substance defined in section 1 (if not read-across):
no
Details on test material:
Alcide Gel is a preparation composed of sodium chlorite and lactic acid, which when combined in equal volumes results in the formation of chlorine dioxide.

Test animals

Species:
rabbit
Strain:
New Zealand White
Sex:
male/female
Details on test animals and environmental conditions:
Forty rabbits (1.57 - 1.64 kg), twenty of each sex were used in the studies.

Administration / exposure

Type of coverage:
no data
Vehicle:
unchanged (no vehicle)
Details on exposure:
No data
Analytical verification of doses or concentrations:
no data
Details on analytical verification of doses or concentrations:
No data
Duration of treatment / exposure:
Duration of treatment: 3 months
Frequency of treatment:
Alcide gel was applied 5 day/week
Doses / concentrations
Doses / concentrations:
0.5, 1.0 and 2.0 g/kg
Basis:
other: Doses were administered on a gel weight basis containing 50 % Part A and 50 % Part B.
No. of animals per sex per dose:
4 rabbits/sex/group
Control animals:
other: Eight animals received 2.0 g/kg of a placebo gel which contains the gelling material alone without the active ingredients. Another group served as the control and did not receive any treatment.
Details on study design:
Any test material remaining on the skin following the daily exposure was washed off prior to the new application.
Positive control:
No data

Examinations

Observations and examinations performed and frequency:
No data
Sacrifice and pathology:
After 3 months, blood was collected from all animals by cardiac puncture. White blood cell count, red blood cell count, haemoglobin concentration, packed cell volume, mean corpuscular volume, mean corpuscular haemoglobin and mean corpuscualr haemoglobin concentration were determined.
Clinical studies were conducted after 90 days. The remainder of the blood was used for the determination of glutathione (GSH), osmotic fragility and methemoglobin.
Organ/ body weight ratios were calculated .
The liver, kidney, lung, heart, ovary/testes, spleen, skin, stomach, duodenum and ileum from all rabbits were examined microscopically while microscopic examination of brain, pancreas, adrenals and thyroid was done only on animals from the high dose and control groups.
Other examinations:
No data
Statistics:
Statistical analysis of food consumption, body weight, haematology, clinical chemistry, glutathione, osmotic fragility and organ/ body weight ratios were performed using an analysis of variance test and Duncan's multiple range test.

Results and discussion

Results of examinations

Clinical signs and mortality:
no effects
Dermal irritation:
no effects
Body weight and weight gain:
no effects
Food consumption:
no effects
Food efficiency:
not examined
Water consumption:
not examined
Ophthalmoscopic examination:
not examined
Haematology:
yes
Clinical chemistry:
yes
Urinalysis:
not examined
Neurobehaviour:
not examined
Organ weights:
yes
Gross pathology:
yes
Histopathology: non-neoplastic:
yes
Histopathology: neoplastic:
not examined
Details on results:
CLINICAL SIGNS
All rabbits appeared healthy throughout the 90 day treatment period. 

DERMAL IRRITATION
No changes were found at physical examination of the application sites during the experiment.

FEED CONSUMPTION AND BODY WEIGHT
These parameters were not significantly altered at any time point.

CLINICAL CHEMISTRY AND HAEMATOLOGY
In the 2.0 g/kg Alcide group as well as in the placebo group, creatinine values were elevated in serum, 1.60 ± 0.06 and 1.64 ± 0.07 vs 1.32 ± 0.08 for the control group, respectively. In addition the blood urea nitrogen/ creatinine ratio was reduced in the 2.0 g/kg group, 11.5 ± 0.8 compared to 14.6 ± 1.1 for the control group. In the 1.0 g/kg Alcide group, the carbon dioxide content was increased in serum while the serum inorganic phosphorous and calcium concentrations were decreased in serum.
No significant changes were noted in experimental aniamls compared to controls for any of the haematological parameters studied.
Glutathione content in blood was significantly decreased in the group receiving 2.0 g/kg Alcide gel as well as in the placebo gel group which also received 2.0 g/kg. Erythrocyte osmotic fragility was not altered and methemoglobin was not detected in blood.

ORGAN WEIGHT
In the group receiving 1.0 g/kg of Alcide gel, the liver/ body weight ration was significantly increased compared to the control group.

PATHOLOGY
All organs appeared normal.

HISTOPATHOLOGY
No histological changes were observed in the livers of either this group or in any other treatment group. Adrenal cortical hyperplasia was observed in all animals examined , including the control group and was the only significant histopathological alteration observed.
Any other information on results incl. tables:
No data

Applicant's summary and conclusion

Executive summary:
In a subchronic toxicity study, Chlorine Dioxide (ClO2) under Alcide gel form, was applicated on the backs of forty male and female New Zealand White rabbits at dose levels of 0.5, 1.0 and 2.0 g/kg bw for three months.
An animal group received 2.0 g/kg bw of a placebo gel which contains the gelling material alone without the active ingredients whereas another animal control group did not received any treatment.
After three months, blood was collected from all animals, clinical studies were conducted, organ/body weight ratios were calculated and several tissues were examined microscopically.
All rabbits appeared healthy at the end of the experiment and no changes were found at physical examination of the application sites during the experiment. Feed consumption and body weights remained stable during the treatment period.
Glutathione concentrations in blood were decreased in the group receiving 2.0 g/kg Alcide gel as well as in the placebo gel group which received the same concentration. The 1.0 and 0.5 g/kg Alcide groups did not have any alterations in glutathione content. This observation suggests that the gel itself was responsible for glutathione depletion.
No significant changes were noted in experimental animals compared to controls for any of the haematological parameters studied.
In the group receiving 1.0 g/kg of Alcide gel, the liver/ body weight ration was significantly increased compared to the control group.
No histological changes were observed in the livers of either this group or in any other treatment group.
In this dermal toxicity study using rabbits, no gross signs of toxicity were observed.

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